HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53998100, compound → HCID 178467693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53998100 | HCID 53998100 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178467693 | HCID 178467693 | — |
Reaction Steps
3.3 g of 2-(3-benzyl-3H-imidazol-4-yl)-4-phenylbutan-2-ol is dissolved in 100 ml of ethanol. The reaction solution is hydrogenated at 50° C. with 10% palladium on carbon as catalyst for 4.5 hours. Work-up of the reaction mixture gives the crude product, which is recrystallized from ethyl acetate. The yield is 2.0 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479530B2 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-68c5e25b555f4281989bdeaecaa0f39c |
| Source note | uspto-grants-2002_11 |