HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 82633711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Bromo-2,5-dimethylbenzoic acid | HCID 2753479 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 82633711 | HCID 82633711 | — |
Reaction Steps
10.3 g (45 mmol) of 4-bromo-2,5-dimethylbenzoic acid are dissolved in 250 ml of dichloromethane and after the addition of 9.9 ml of (135 mmol) of thionyl chloride refluxed for two hours. Then the mixture is evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479524B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-18404acdd5ac40eea2a7fb1202460710 |
| Source note | uspto-grants-2002_11 |