HCID 10113742, compound → HCID 10136885, compound

HRID 1017892Notes

Reaction equation

HRID 1017892 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:29])=[C:16]([NH:21][C:22]([C:24]4[S:25][CH:26]=[CH:27][CH:28]=4)=O)[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][C:11]2([CH3:31])[CH3:30])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>CO>[CH:1]([C:4]1[CH:5]=[CH:6][C:7]([CH:10]2[C:14]3[C:15]([CH3:29])=[C:16]([NH:21][CH2:22][C:24]4[S:25][CH:26]=[CH:27][CH:28]=4)[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][C:11]2([CH3:31])[CH3:30])=[CH:8][CH:9]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 10113742HCID 10113742, compound

Product 1

HCID 10136885HCID 10136885, compoundYield 61%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

By using N-[3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-2-thiophenecarboxamide, the title compound was synthesized according to Example 2b. Yield: 61%. Melting point: 101-103° C. (Methanol)

Sources & evidence

ORD record
ord-f9362813cbe04dd1adebe663f97e2397
Source dataset
uspto-grants-2002_11
Patent number
US06479536B1

Reaction notes

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