HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 10181308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | HCID 10828013 | HCID 10828013 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 10181308 | HCID 10181308 | 79% |
Reaction Steps
By using 3-(4-fluorophenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-amine and 4-methoxybenzoyl chloride, the title compound was synthesized according to Example 1b. Yield: 79%. Melting point: 191-194° C. (Ethyl acetate-hexane)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479536B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-82c4fbca1f37460fb8227c455207479f |
| Source note | uspto-grants-2002_11 |