HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-(chlorocarbonyl)benzoate → HCID 21961308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-(chlorocarbonyl)benzoate | HCID 81850 | — |
| Reactant | 3-(4-Isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-amine | HCID 10519978 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21961308 | HCID 21961308 | 92% |
Reaction Steps
By using 3-(4-isopropylphenyl)-2,2,4,6,7- pentamethyl-2,3-dihydro-1-benzofuran-5-amine and 4-methoxycarbonylbenzoyl chloride, the title compound was synthesized according to Example 1b. Yield: 92%. Melting point: 220-223° C. (Methanol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479536B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-ceecca4110b64f8db573ce41ec4ef298 |
| Source note | uspto-grants-2002_11 |