HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzoyl chloride → 4-Fluoro-N-(2,4,6,7-tetramethyl-3-phenyl-5-benzofuranyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Reactant | HCID 68886540 | HCID 68886540 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 4-Fluoro-N-(2,4,6,7-tetramethyl-3-phenyl-5-benzofuranyl)benzamide | HCID 10293579 | 80% |
Reaction Steps
By using 2,4,6,7-tetramethyl-3-phenyl-1-benzofuran-5-amine and 4-fluorobenzoyl chloride, the title compound was synthesized according to Example 1b. Yield: 80%. Melting point: 242-245° C. (Ethyl acetate-hexane)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479536B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-ada766b3d4934b66b40cd9a9ec1c0bcd |
| Source note | uspto-grants-2002_11 |