Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | Decyl acrylate | HCID 16541 | — |
| Reactant | Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1) | HCID 162071 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | n-Decylacrylate Acrylamide | HCID 86584090 | — |
Reaction Steps
To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux condenser, and septum was added 150 mL of isopropanol followed by 16.13 g of a 50% aqueous solution of 2-trimethylammonioethylacrylate chloride, 8.06 g of n-decylacrylate, and 8.06 g of acrylamide. The solution was purged with nitrogen for 1 hour and 0.5 g AIBN was added. The mixture was purged for ˜15 minutes until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06482402B1 |
|---|
| Source dataset | uspto-grants-2002_11 |
|---|
| ORD ID | ord-e485583c4a5f4ab78b7051e1895403a5 |
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| Source note | uspto-grants-2002_11 |
|---|
