Benzyl Chloride → HCID 178462733, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 625 g of a 20.0 wt. % solution of styrene-co-1-vinylimidazole (50/50) in DMF was quaternized with benzyl chloride as described for the preparation of compound F-4, except that 15.9 g of benzyl chloride was used. Following heating and stirring at 100° C. for 18 hr the reaction mixture was cooled and the polymer precipitated into diethyl ether with rapid stirring. The flaky precipitate was washed well with diethyl ether and dried in a vacuum oven.

Provenance & Evidence