HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzoylbenzoic Acid → HCID 178518893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzoylbenzoic Acid | HCID 6813 | — |
| Reactant | Hydrazine | HCID 9321 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178518893 | HCID 178518893 | — |
Reaction Steps
The mixture of o-benzoyl benzoic acid (11.3 g; 0.05 mol) and hydrazine (0.15 mol) in ethanol (150 ml) is stirred at room temperature for 5-24 hours to give 1-hydroxy-4-phenyl phthalazine as a white precipitate which is filtered off and is washed with ethanol. (12.3 g)(m.p. 240° C.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06486158B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-23b836e8b43b47abb61e6d678e4dfe9f |
| Source note | uspto-grants-2002_11 |