HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(O-Benzylhydroxylamino)-3-chloro-2-ethylpyridine → 4-[O-Benzyl-N-(spiro[5.5]undecan-3-yl)hydroxylamino]-3-chloro-2-ethylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(O-Benzylhydroxylamino)-3-chloro-2-ethylpyridine | HCID 19693937 | — |
| Reactant | 3-Tosyloxyspiro[5.5]undecane | HCID 19694044 | — |
| Product | 4-[O-Benzyl-N-(spiro[5.5]undecan-3-yl)hydroxylamino]-3-chloro-2-ethylpyridine | HCID 19693962 | 95% |
Reaction Steps
Was prepared analogously to Example 7 from 4-(O-benzylhydroxylamino)-3-chloro-2-ethylpyridine (Example 52) and 3-tosyloxyspiro[5.5]undecane. Yield: 95%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723450 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-aef921fb8b7c405c92fb8244dd4e6640 |
| Source note | uspto-grants-1998_03 |