HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54300444, compound → HCID 56979361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54300444 | HCID 54300444 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 56979361 | HCID 56979361 | 59.7% |
Reaction Steps
4,4-Dimethylcholesta-5,8-diene-3-one (100 mg) is reduced with lithiumaluminumhydride (5 mg) in 2 ml tetrahydrofuran at room temperature. The solution is stirred for one hour. After aqueous work-up and column chromatography 4,4-dimethylcholesta-5,8-diene-3β-ol (60 mg) is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06486145B2 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-5159581bbab6453f8f73b614b2523d15 |
| Source note | uspto-grants-2002_11 |