HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23278998, compound → HCID 18400131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23278998 | HCID 23278998 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18400131 | HCID 18400131 | 98.6% |
Reaction Steps
A solution of 3,5-dimethyl-2,4-dinitroaniline (1.5 g, 7 mmol) in ethyl acetate (100 mL) is treated with hydrogen at atmospheric pressure for 2 hours. The mixture is filtered on Celite and the filtrate is rotary evaporated to afford 1,2-diamino-3,5-dimethyl4-nitrobenzene (1.25 g) as a red solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06486190B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-adddc5e8f53c40ea88ae20d33fc2f6f0 |
| Source note | uspto-grants-2002_11 |