HRID1019436

反应详情

EQUATION

反应方程式

HRID 1019436 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1-Hexyl-3-methylimidazolium chloride (10 g, 0.0493 moles) was mixed with reagent-grade acetone (100 ml) in a large round-bottomed flask and stirred vigorously under a nitrogen blanket. Potassium 1,1,2,2-tetrafluoroethane sulfonate (TFES-K, 10 g, 0.0455 moles) was added to reagent grade acetone (100 ml) in a separate round-bottomed flask, and this solution was carefully added to the 1-hexyl-3-methylimidazolium chloride/acetone mixture. The mixture was left to stir overnight. The reaction mixture was then filtered using a large frit glass funnel to remove the white KCl precipitate formed, and the filtrate was placed on a rotary evaporator for 4 hours to remove the acetone.

WORKUP

后处理

  1. waitThe mixture was left
  2. stirringto stir overnight
  3. filtrationThe reaction mixture was then filtered
  4. customto remove the white KCl precipitate
  5. customformed
  6. customthe filtrate was placed on a rotary evaporator for 4 hours
  7. customto remove the acetone