HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Acrylic acid vinylpyrrolidone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| Solvent | 1-Methoxy-2-propanol | HCID 7900 | — |
| Product | Acrylic acid vinylpyrrolidone | HCID 197163 | — |
Reaction Steps
58.5 g of vinylpyrrolidone (P-6-1), 70.5 g of acrylic acid (P-6-2), and 9.0 g azobisisobutyronitrile were dissolved in propylene glycol monomethyl ether and reacted at 80° C. for 9 hours to polymerize monomers. The polymerization product was purified by precipitation from hexane to obtain 110 g of a poly(acrylic acid/vinylpyrrolidone) copolymer with an Mw of 5,600 and Mw/Mn of 1.62. This copolymer is indicated as a resin P-6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08715901B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-4b81e6e0b95a4924bcf721e96630daee |
| Source note | uspto-grants-2014_05 |