Hydrochloric Acid → HCID 66907679, compound

Participants

Reaction Steps

2.6 mL of a 2M solution of hydrochloric acid is added to a solution of 1.2 g of N-[6-(azetidin-1-yl)pyridin-3-yl]-5-trifluoromethyl-1-(3-fluorobenzyl)-1H-pyrrolo[2,3-b]pyridine-2-carboxamide, prepared in the preceding stage, in 50 mL of dichloromethane. The solution is concentrated to dryness and the resultant solid is recrystallized from ethanol. In this way we isolate 0.62 g of the expected salt.

Provenance & Evidence