HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1-[2-(4-Chloroanilino)anilino]-3-fluoro-4,6-dinitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,5-Difluoro-2,4-dinitrobenzene | HCID 67598 | — |
| Reactant | N-(4-chlorophenyl)benzene-1,2-diamine | HCID 522323 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-[2-(4-Chloroanilino)anilino]-3-fluoro-4,6-dinitrobenzene | HCID 71503881 | — |
Reaction Steps
The solid from step B was added to a solution of 1,3-difluoro-4,6-dinitrobenzene (46 g) in methanol (200 mL), then triethylamine (31.4 mL) was added, and stirred at rt for 4 h. The reaction mixture was filtered, and the cake was washed with methanol to give 80.6 g of red solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716292B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-a0b26f8a19b44080a56c6d12186e3245 |
| Source note | uspto-grants-2014_05 |