Acetyl chloride → HCID 49787469, compound

Participants

Reaction Steps

CO-AAW0003 (39 mgs, 0.12 mmoles) was dissolved in anhydrous dimethylacetamide (1 ml) followed by the addition of triethylamine (20 ul, 0.144 mmols) and acetyl chloride (10.3 ul, 0.144 mmoles). The reaction was then left stirring at room temperature for 1.5 hours. The reaction was purified by C18 reverse phase automated HPLC (21 mgs, 67% yield, 100% pure, CO-AAW00024).

Provenance & Evidence