Cyclohexylamine → HCID 52917269, compound

HRID 1020170Notes

Reaction equation

HRID 1020170 reaction equation
CS([C:5]1[N:10]=[CH:9][C:8]([C:11]#[C:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:7][N:6]=1)(=O)=O.[CH:19]1([NH2:25])[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH:19]1([NH:25][C:5]2[N:10]=[CH:9][C:8]([C:11]#[C:12][C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)=[CH:7][N:6]=2)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 7965CyclohexylamineHCID 575167582-Methanesulfonyl-5-phenylethynyl-pyrimidine

Product 1

HCID 52917269HCID 52917269, compound

Procedure

The title compound, white solid, MS: m/e=278.2 (M+H+), can be prepared in accordance with the general method of example 1, step 3 from 2-methanesulfonyl-5-phenylethynyl-pyrimidine (example 1, step 2) and cyclohexanamine.

Sources & evidence

ORD record
ord-1726aa188dfe47e2aee0cf4f4abb7cba
Source dataset
uspto-grants-2014_05
Patent number
US08716316B2

Reaction notes

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