Phenylacetylene → HCID 57517075, compound

HRID 1020181Notes

Reaction equation

HRID 1020181 reaction equation
[CH:1]1([O:7][C:8]2[CH:13]=[CH:12][C:11](I)=[CH:10][N:9]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:15]1([C:21]#[CH:22])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH:1]1([O:7][C:8]2[CH:13]=[CH:12][C:11]([C:22]#[C:21][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[CH:10][N:9]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 10821PhenylacetyleneHCID 425531502-(Cyclohexyloxy)-5-iodopyridine

Product 1

HCID 57517075HCID 57517075, compound

Procedure

The title compound, brown oil, MS: m/e=278.1 (M+H+), can be prepared in accordance with the general method of example 18, step 2 from 2-(cyclohexyloxy)-5-iodopyridine and phenylacetylene.

Sources & evidence

ORD record
ord-30851fc111fc4dcc86ba18a145949135
Source dataset
uspto-grants-2014_05
Patent number
US08716316B2

Reaction notes

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