2-Chloro-5-nitropyridine → HCID 57461801, compound

HRID 1020356Notes

Reaction equation

HRID 1020356 reaction equation
Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-])=O)=[CH:4][N:3]=1.[CH2:11]([CH:19]1[CH2:24][CH2:23][NH:22][CH2:21][CH2:20]1)[CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH2:11]([CH:19]1[CH2:20][CH2:21][N:22]([C:2]2[N:3]=[CH:4][C:5]([NH2:8])=[CH:6][CH:7]=2)[CH2:23][CH2:24]1)[CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 783082-Chloro-5-nitropyridineHCID 43418954-(2-Phenylethyl)piperidine

Product 1

HCID 57461801HCID 57461801, compound

Procedure

Intermediate B-22 was prepared by the general procedure for intermediate B-2, by using 2-chloro-5-nitropyridine and 4-phenethylpiperidine as starting materials. MS (M+1): 312.

Workup

  1. customIntermediate B-22 was prepared by the general procedure for intermediate B-2

Sources & evidence

ORD record
ord-1a7cfbb924a34ae7a88e004e00a8016f
Source dataset
uspto-grants-2014_05
Patent number
US08716312B2

Reaction notes

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