2-Chloro-5-nitropyridine → HCID 57461802, compound

HRID 1020357Notes

Reaction equation

HRID 1020357 reaction equation
Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-])=O)=[CH:4][N:3]=1.[CH2:11]([O:18][CH:19]1[CH2:24][CH2:23][NH:22][CH2:21][CH2:20]1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:18][CH:19]1[CH2:24][CH2:23][N:22]([C:2]2[N:3]=[CH:4][C:5]([NH2:8])=[CH:6][CH:7]=2)[CH2:21][CH2:20]1)[C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 783082-Chloro-5-nitropyridineHCID 31574604-(Benzyloxy)piperidine

Product 1

HCID 57461802HCID 57461802, compound

Procedure

Intermediate B-23 was prepared by the general procedure for intermediate B-2, by using 2-chloro-5-nitropyridine and 4-benzyloxypiperidine as starting materials. MS (M+1): 284.

Workup

  1. customIntermediate B-23 was prepared by the general procedure for intermediate B-2

Sources & evidence

ORD record
ord-849c38bf5e7e4cf5b70253d2255ae3aa
Source dataset
uspto-grants-2014_05
Patent number
US08716312B2

Reaction notes

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