2-Chloro-5-nitropyridine → HCID 67391195, compound

HRID 1020359Notes

Reaction equation

HRID 1020359 reaction equation
Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-])=O)=[CH:4][N:3]=1.[C:11]1([CH2:17][NH:18][S:19]([CH:22]2[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]2)(=[O:21])=[O:20])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([CH2:17][NH:18][S:19]([CH:22]2[CH2:27][CH2:26][N:25]([C:2]3[N:3]=[CH:4][C:5]([NH2:8])=[CH:6][CH:7]=3)[CH2:24][CH2:23]2)(=[O:21])=[O:20])[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1

Participants

3

Reactant 2

HCID 783082-Chloro-5-nitropyridineHCID 57767438HCID 57767438, compound

Product 1

HCID 67391195HCID 67391195, compound

Procedure

Intermediate B-25 was prepared by the general procedure for intermediate B-2, by using 2-chloro-5-nitropyridine and 4-((phenylmethylamino)sulfonyl)piperidine as starting materials. MS (M+1): 347.

Workup

  1. customIntermediate B-25 was prepared by the general procedure for intermediate B-2

Sources & evidence

ORD record
ord-710dd78e35454b49a0ef26cd4464bbe9
Source dataset
uspto-grants-2014_05
Patent number
US08716312B2

Reaction notes

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