Phenylmethanesulfonyl chloride → HCID 67389422, compound

Participants

Reaction Steps

Compound 41 was prepared by the general procedure for compound 8, by using compound 39 and α-toluenesulfonyl chloride as starting materials. 1H NMR (500 MHz, CDCl3) δ 8.10 (d, 1H, J=2.5 Hz), 7.85 (dd, 1H, J=2.5, 9 Hz), 7.50 (s, 1H), 7.40 (m, 3H), 7.35 (m, 2H), 6.50 (d, 1H, J=9 Hz), 4.25 (s, 2H), 4.10 (m, 2H), 3.75 (m, 4H), 3.20 (m, 2H), 3.05 (t, 1H, J=9.5 Hz), 2.95 (t, 1H, J=6 Hz), 2.75 (t, 1H, J=11 Hz), 1.60-2.00 (m, 6H), 1.20 (q, 1H, J=11 Hz), 1.00 (d, 3H, J=7 Hz). MS (M+1): 607.

Provenance & Evidence