Hydroxyamine hydrochloride → HCID 49805674, compound

Participants

Reaction Steps

The procedure of the step 3 in Example 80 was repeated except that 6-(2-methyl-3-phenyl-benzamido)hexanoic acid (38 mg, 0.116 mmol)) instead of 6-(3-bromo-2-methylbenzamido)hexanoic acid and hydroxylamine hydrochloride (16 mg, 0.23 mmol) instead of 1,2-phenylenediamine were used and purified by a preparative HPLC (C18, 20% H2O/CH3CN, 20 ml/min) to obtain the title compound (8 mg, 20%).

Provenance & Evidence