Hydroxyamine hydrochloride → HCID 49805796, compound

Participants

Reaction Steps

The procedure of the step 3 in Example 80 was repeated except that 6-(3-methyl-4-phenyl-benzamido)hexanoic acid (70 mg (0.215 mmol)) instead of 6-(3-bromo-2-methylbenzamido)hexanoic acid, and 30 mg of hydroxylamine hydrochloride (0.43 mmol) instead of 1,2-phenylenediamine were used and purified by a preparative HPLC (C18, 20% H2O/CH3CN, 20 ml/min) to obtain the title compound (38 mg, 51%).

Provenance & Evidence