HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-5-methylpyridine → HCID 57950421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-5-methylpyridine | HCID 564216 | — |
| Reactant | 2-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine | HCID 44754862 | — |
| Product | HCID 57950421 | HCID 57950421 | 42.2% |
Reaction Steps
2-Bromo-5-methylpyridine (2.93 g, 17.0 mmol) and 2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine (3.34 g, 14.2 mmol) were reacted according to Example 31 (step a) to provide the title compound (1.2 g, 42%) as a brown solid: ESI MS m/z 201 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716308B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-ad444a2bf6f245b2b02bc640be1b97d6 |
| Source note | uspto-grants-2014_05 |