HuagongsheHuagongshe Chemistry Print Report · For research reference only
Adipic Acid → 6-Oxohexanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Adipic Acid | HCID 196 | — |
| Reactant | Biphenyl | HCID 7095 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Product | 6-Oxohexanoic acid | HCID 440918 | 18% |
Reaction Steps
After the reaction, the autoclave was cooled with ice, and the pressure was reduced; subsequently, the contents were treated with diazomethane, and the reaction mixture was analyzed by gas chromatography using biphenyl as an internal standard. The results confirmed that adipic acid was obtained in a yield of 38%, and 6-oxohexanoic acid was obtained in a yield of 18%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716501B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-29f1e2e5e0f04bef80ccd49d73fd436e |
| Source note | uspto-grants-2014_05 |