HRID1021233

反应详情

EQUATION

反应方程式

HRID 1021233 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
60 °C

PROCEDURE

实验过程

2,5-Dibromo-1,3-thiazole (500 mg) was mixed with morpholine (2 ml), followed by stirring at 60° C. for 5 hours. Water was added to the reaction mixture, followed by stirring for 1 hour, and the resulting insoluble matter was collected by filtration, followed by washing with water, to obtain 4-(5-bromo-1,3-thiazol-2-yl)morpholine (475 mg).

WORKUP

后处理

  1. stirringby stirring for 1 hour
  2. filtrationthe resulting insoluble matter was collected by filtration
  3. washby washing with water