HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86684458, compound → HCID 86684459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86684458 | HCID 86684458 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 86684459 | HCID 86684459 | 88% |
Reaction Steps
A mixture of 243d (2.2 g, 4.88 mmol) and trifluoroacetic acid (20 mL) was stirred at room temperature for 1 h. It was then concentrated under reduced pressure to afford crude 243e (1.5 g, 88%), which was used in the next step without further purification. MS-ESI: [M+H]+ 352.2
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716274B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-5bca4a5036d042db8a2a0b9c2fc54964 |
| Source note | uspto-grants-2014_05 |