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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1022043Generated: November 1, 2026

HCID 86684458, compound → HCID 86684459, compound

https://huagongshe.com/reaction/1022043

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86684458HCID 86684458—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 86684459HCID 8668445988%

Reaction Steps

A mixture of 243d (2.2 g, 4.88 mmol) and trifluoroacetic acid (20 mL) was stirred at room temperature for 1 h. It was then concentrated under reduced pressure to afford crude 243e (1.5 g, 88%), which was used in the next step without further purification. MS-ESI: [M+H]+ 352.2

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08716274B2
Source datasetuspto-grants-2014_05
ORD IDord-5bca4a5036d042db8a2a0b9c2fc54964
Source noteuspto-grants-2014_05