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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1023049Generated: October 29, 2026

HCID 59625758, compound → HCID 59625748, compound

https://huagongshe.com/reaction/1023049

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59625758HCID 59625758—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
ProductHCID 59625748HCID 59625748160.9%

Reaction Steps

A mixture of compound 8e (1.7 g, 2.9 mmol), and 10% Palladium on carbon (300 mg) was hydrogenated (50 psi hydrogen gas) using a Parr apparatus for 18 h. The catalyst was removed by filtration, and the solvent concentrated under reduced pressure to afford crude compound 8f (1.5 g). MS m/z (M+H+) 322.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722658B2
Source datasetuspto-grants-2014_05
ORD IDord-495456a3f8b84c8882744a94727e911c
Source noteuspto-grants-2014_05