HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59625758, compound → HCID 59625748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59625758 | HCID 59625758 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 59625748 | HCID 59625748 | 160.9% |
Reaction Steps
A mixture of compound 8e (1.7 g, 2.9 mmol), and 10% Palladium on carbon (300 mg) was hydrogenated (50 psi hydrogen gas) using a Parr apparatus for 18 h. The catalyst was removed by filtration, and the solvent concentrated under reduced pressure to afford crude compound 8f (1.5 g). MS m/z (M+H+) 322.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722658B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-495456a3f8b84c8882744a94727e911c |
| Source note | uspto-grants-2014_05 |