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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1023067Generated: October 31, 2026

Potassium Carbonate → HCID 49763995, compound

https://huagongshe.com/reaction/1023067

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 59625903HCID 59625903—
SolventAcetonitrileHCID 6342—
ProductHCID 49763995HCID 49763995139%

Reaction Steps

To a suspension of compound 17a (100 mg) and K2CO3 (69 mg) in MeCN was added compound 18a (0.0353 mL) and the mixture was stirred at room temperature for 30 min. The reaction was concentrated and the residue was diluted with EtOAc and water. The organics were concentrated and purified by flash column chromatography (silica gel, 8% MeOH/EtOAc) to afford compound 355 (85 mg). MS m/z (M+H+) 495.6.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722658B2
Source datasetuspto-grants-2014_05
ORD IDord-16d7dd1137d94000a4117857e7d014eb
Source noteuspto-grants-2014_05