HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hydroxycyclohexanecarboxylic acid → HCID 178523687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hydroxycyclohexanecarboxylic acid | HCID 219640 | — |
| Reactant | HCID 178478587 | HCID 178478587 | — |
| Product | HCID 178523687 | HCID 178523687 | — |
Reaction Steps
The title compound, white solid (20 mg, 61%), MS (ISP) m/z=458.3 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperazin-1-yl)-ethyl]-cyclohexylamine trihydrochloride (Intermediate A) (30 mg, 68.1 mmol) and 1-hydroxycyclohexanecarboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722683B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-91f9b9ddde0f4021b427a8f9d9772e8e |
| Source note | uspto-grants-2014_05 |