HuagongsheHuagongshe Chemistry Print Report · For research reference only
(-)-2-Hydroxy-3-methylbutyric acid → HCID 178448392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (-)-2-Hydroxy-3-methylbutyric acid | HCID 5289545 | — |
| Reactant | HCID 178478587 | HCID 178478587 | — |
| Product | HCID 178448392 | HCID 178448392 | — |
Reaction Steps
The title compound, white solid (12.1 mg, 34.4%), MS (ISP) m/z=432.4 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperazin-1-yl)-ethyl]-cyclohexylamine hydrochloride (Intermediate A) (30 mg, 81.5 mmol) and (R)-2-hydroxy-3-methylbutanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722683B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-1335fd8dffbb45ba8a992d4d8493654d |
| Source note | uspto-grants-2014_05 |