Morpholine-4-sulfonyl chloride → HCID 178527581, compound

Participants

Reaction Steps

The title compound, white solid (24.6 mg, 60.2%), MS (ISP) m/z=481.2 [(M+H)+], was prepared in accordance with the general method of example 76 from N-trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperazin-1-yl)-ethyl]-cyclohexylamine hydrochloride (Intermediate A) (30 mg, 81.5 μmol) and morpholine-4-sulfonyl chloride.

Provenance & Evidence