Potassium Carbonate → HCID 56968080, compound

Participants

Reaction Conditions

Reaction Steps

To the crude 1-benzoyl-3-[4-(2-o-tolyl-ethyl)-pyridin-2-yl]-urea (225 mg, 0.63 mmol) in ethanol (2 mL) is added potassium carbonate (86 mg, 0.63 mmol). The resulting mixture is heated at 85° C. for 30 min. Solvent is removed and the residue is purified by silica flash column chromatography eluting with EtOAc in Heptane (gradient from 0% to 100%) to give 60 mg of the titled product.

Provenance & Evidence