HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-aminobenzoate → Ethyl 3-[(4,5-diisopropylfuran-2-carbonyl)amino]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-aminobenzoate | HCID 11400 | — |
| Reactant | 4,5-Diisopropylfuran-2-carboxylic acid | HCID 58420514 | — |
| Product | Ethyl 3-[(4,5-diisopropylfuran-2-carbonyl)amino]benzoate | HCID 67394561 | 89% |
Reaction Steps
In the same manner as that of Example 2, 4,5-diisopropylfuran-2-carboxylic acid (60 mg, 0.306 mmol) was condensed with ethyl 3-aminobenzoate, and the resultant was purified by silica gel chromatography [hexane-ethyl acetate (7:2)] to obtain ethyl 3-[(4,5-diisopropylfuran-2-carbonyl)amino]benzoate (93 mg, 89%) as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722730B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-851ed1bc365c4d25a556b6aeb91b712a |
| Source note | uspto-grants-2014_05 |