HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-amino-o-anisate → HCID 67394461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-amino-o-anisate | HCID 168705 | — |
| Reactant | 4,5-Diisopropylfuran-2-carboxylic acid | HCID 58420514 | — |
| Product | HCID 67394461 | HCID 67394461 | 45% |
Reaction Steps
In the same manner as that of Example 24, 4,5-diisopropylfuran-2-carboxylic acid (80 mg, 0.408 mmol) and methyl 2-methoxy-4-aminobenzoate (133 mg, 0.734 mmol) were condensed, the reaction mixture was treated in a conventional manner, and then the residue was purified by silica gel chromatography [hexane-ethyl acetate (5:1)] to obtain methyl 2-methoxy-4-[(4,5-diisopropylfuran-2-carbonyl)amino]benzoate (65 mg, 45%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722730B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-f95bea03c7d242f4adb762907280d39e |
| Source note | uspto-grants-2014_05 |