Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1023917Generated: October 30, 2026

5-Bromo-2-nitropyridine → HCID 59191356, compound

https://huagongshe.com/reaction/1023917

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Bromo-2-nitropyridineHCID 817620—
ReactantHCID 59191405HCID 59191405—
ProductHCID 59191356HCID 59191356103.3%

Reaction Steps

According to the procedure of example 20(a), except substituting 1-fluoro-4-nitro-2-(trifluoromethyl)benzene for 5-bromo-2-nitropyridine (406 mg, 2 mmol), the title compound (220 mg; 38%) was prepared as a white solid, after chromatography on silica gel (gradient cyclohexane/dichloromethane), along with 5-bromo-2-(2-methoxy-4-propylphenoxy)pyridine (238 mg; 37%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722746B2
Source datasetuspto-grants-2014_05
ORD IDord-a59aaa795b084b9f8a13d1f48bccdaee
Source noteuspto-grants-2014_05