HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59191266, compound → HCID 59191419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59191266 | HCID 59191266 | — |
| Reactant | HCID 59191318 | HCID 59191318 | — |
| Reactant | HCID 59191398 | HCID 59191398 | — |
| Product | HCID 59191419 | HCID 59191419 | 19% |
Reaction Steps
According to the procedure of example 5(b), except substituting 2-fluoro-6-(2-methoxy-4-propylphenoxy)pyridine for a mixture of 4-(4-ethyl-2-methoxyphenoxy)-2-fluoroaniline and 2-(4-ethyl-2-methoxyphenoxy)-4-fluoroaniline (50.9 mg, 0.19 mmol), the title compound (8.9 mg; 19%) was obtained after purification by preparative TLC (dichloromethane/ethyl acetate: 9/1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722746B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-19f8565ec01c4ce395408f8dba360449 |
| Source note | uspto-grants-2014_05 |