Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1023974Generated: October 30, 2026

Tetrahydrofuran → HCID 59191395, compound

https://huagongshe.com/reaction/1023974

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrahydrofuranHCID 8028—
ReactantHCID 59191339HCID 59191339—
SolventEthanolHCID 702—
ProductHCID 59191395HCID 5919139562%

Reaction Steps

According to the procedure of example 20(b) except substituting 4-ethyl-2-methoxy-1-[4-nitro-2-(trifluoromethyl)phenoxy]benzene for 4-(2-Benzyloxy-4-ethyl-phenoxy)-3-fluoro-N-(2-pyridin-2-yl-ethyl)-benzene sulfonamide (150 mg; 0.30 mmol) and tetrahydrofurane for ethanol (3 mL), the title compound (70 mg; 62%) was obtained as a clear oil, after purification via preparative TLC (dichloromethane/ethyl acetate).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722746B2
Source datasetuspto-grants-2014_05
ORD IDord-208a897b0ba545ed874db5f70aa18755
Source noteuspto-grants-2014_05