Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Indene | HCID 7219 | — |
| Reactant | Alpha-Methylstyrene | HCID 7407 | — |
| Product | HCID 6713780 | HCID 6713780 | — |
Reaction Steps
A resin J-1 is prepared in a manner similar to that of preparing the resin I-1, except that 72 g of α-methylstyrene and 18 g of indene (that is, α-methylstyrene: 80 mass %, indene: 20 mass %) are used and that the addition of the catalyst is carried for 15 minutes and the polymerization reaction is allowed to proceed for 1 hour in a state where the temperature of the reaction mixed solution is maintained in the range of 13 to 15° C. The α-methylstyrene/indene copolymer resin thus obtained has yield: 77 g, softening point: 145° C., number-average molecular weight (Mn): 800, and weight-average molecular weight (Mw): 2000.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08722806B2 |
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| Source dataset | uspto-grants-2014_05 |
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| ORD ID | ord-a79c03858d494842bfd8dafe49829354 |
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| Source note | uspto-grants-2014_05 |
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