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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1024164Generated: October 29, 2026

1H-Pyrrolo(2,3-b)pyridine → HCID 178526243, compound

https://huagongshe.com/reaction/1024164

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1H-Pyrrolo(2,3-b)pyridineHCID 9222—
Reactantm-Chloroperbenzoic acidHCID 70297—
Solvent1,2-DimethoxyethaneHCID 8071—
ProductHCID 178526243HCID 178526243—

Reaction Steps

1H-Pyrrolo[2,3-b]pyridine 7-oxide 23 was synthesized by reacting commercially available 7-azaindole 1 with an oxidizing agent (e.g. m-CPBA) in a non-reactive solvent (e.g. dimethoxyethane) as described by Schneller, S. W.; Luo, Jiann-Kuan. J. Org. Chem. 1980, 45:4045-4048. The compound was isolated by filtration of the resulting solid that forms upon standing at 5° C. for typically 1-3 h.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722702B2
Source datasetuspto-grants-2014_05
ORD IDord-684f120809d74c35b415b26633feaccf
Source noteuspto-grants-2014_05