HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 149159545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 152782811 | HCID 152782811 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 149159545 | HCID 149159545 | — |
Reaction Steps
4.6 0.1 ml of thionyl chloride is added to a suspension of 200 mg of “4e” in 4 ml of THF, and the mixture is stirred for a further hour. 3 ml of toluene are added, and the solvents are removed at 300, giving 5-chlorocarbonyl-6-hydroxy-3-(3-methylbenzyl)-1H-indazole (“4f”)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722903B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-3e38fbc58af54b4f8a1d860266622447 |
| Source note | uspto-grants-2014_05 |