HCID 59775159, compound → HCID 59775156, compound

Participants

Reaction Steps

10 g of 4-(4-fluoro-benzyloxy)-2-nitro-aniline or 4-(4-Fluoro-benzyloxy)-1,2-dinitrobenzene was dissolved in 800 ml of methanol and 2 g of Raney Nickel was added. The resulting mixture was hydrogenated at room temperature under regular pressure for 5 hours. The reaction mixture was filtered with celite and washed with methanol. The filtrate was evaporated in vacuo to dryness to give the brown product, which gradually become black, in a quantitative yield.

Provenance & Evidence