HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-(Trifluoromethoxy)phenol → HCID 86665954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-(Trifluoromethoxy)phenol | HCID 70015 | — |
| Reactant | Ethyl 2,6-dichloronicotinate | HCID 12263987 | — |
| Product | HCID 86665954 | HCID 86665954 | 829.4% |
Reaction Steps
2,6-dichloronicotinic acid ethyl ester (0.22 g, 0.1 mmol) and 4-trifluoromethoxy-phenol (0.178 g, 0.1 mmol) were coupled using the procedure of Example 17(a) to afford 0.3 g of the required produCt. Percentage purity (LCMS): 64.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-a36f40e1fb1b4e1dbd607af5a6c56df2 |
| Source note | uspto-grants-2014_05 |