HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Aminoethyl)piperidine, 4-BOC protected → HCID 66818731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Aminoethyl)piperidine, 4-BOC protected | HCID 1501849 | — |
| Reactant | HCID 66818161 | HCID 66818161 | — |
| Product | HCID 66818731 | HCID 66818731 | 69.8% |
Reaction Steps
2-(4-cyano phenoxy)-6-(4-trifluoromethoxy phenoxy)nicotinic acid (0.2 g, 0.48 mmol) and (2-Piperidin-4-yl-ethyl)-carbamic acid tert-butyl ester (0.11 g, 0.48 mmol) were coupled using the procedure of Example 5(c) to afford 0.21 g of the required product. Percentage purity (LCMS): 68.11%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-95e5569b5d6a408a88df5a689d5cfcb0 |
| Source note | uspto-grants-2014_05 |