HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,3,4-Tetrahydroquinoline → HCID 86665956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,3,4-Tetrahydroquinoline | HCID 69460 | — |
| Reactant | HCID 66818818 | HCID 66818818 | — |
| Product | HCID 86665956 | HCID 86665956 | 82.1% |
Reaction Steps
Following the procedure of Example 5(c) 3,5-bis-(4-cyano-phenoxy)-benzoic acid 1.2 g (3.36 mmol) and 1,2,3,4-tetrahydro-quinoline (0.44 g, 3.36 mmol) were used to afford 1.3 g of the required product. 1H NMR (DMSO-d6): δ 1.92 (2H, t), 2.54 (2H, m) 3.75 (2H, t), 6.92 (2H, d), 7.08 (7H, m), 7.82 (4H, d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-3c8159aafff641778855900ebf089c45 |
| Source note | uspto-grants-2014_05 |