Ethyl 4-(bromomethyl)benzoate → HCID 67606146, compound

Participants

Reaction Steps

Using 1.2 g (2.65 mmol) of {4-[3-(4-cyano-phenoxy)-5-hydroxy-benzoylamino]-cyclohexyl}-carbamic acid tert-butyl ester and 4-bromomethyl-benzoic acid ethyl ester (0.644 g, 2.65 mmol) and following the procedure of Example 42(b) afforded 1.32 g of the required product. Percentage purity (LCMS): 84.4%, (M+1)=613.2+1.

Provenance & Evidence