HuagongsheHuagongshe Chemistry Print Report · For research reference only
Decahydroquinoline → HCID 66818895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Decahydroquinoline | HCID 92911 | — |
| Reactant | HCID 66818647 | HCID 66818647 | — |
| Product | HCID 66818895 | HCID 66818895 | 72.4% |
Reaction Steps
3-(4-Cyano-phenoxy)-5-hydroxy-benzoic acid (1.5 g, 5.87 mmol) and decahydro-quinoline (0.89 g, 6.45 mmol) and other reagents as described in Example 9(e) were used to afford 1.6 g of the required product. NMR (DMSO-d6): δ 1.35 (6H, m), 1.80 (7H, m), 3.0 (1H, m), 3.6 (1H, m), 4.5 (1H, m), 6.44 (1H, s), 6.54 (2H, m), 7.16 (2H, d), 7.88 (2H, d), 10.1 (1H, brs).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-c3e95a3c257f499d9a0ff33974e470a1 |
| Source note | uspto-grants-2014_05 |