[3,5-Bis-(4-cyano-phenoxy)-phenyl]-amine → HCID 178453961、化合物

関与物質

反応手順

Following the procedure of Example 9(e) cis-4-tert-butoxycarbonylamino-cyclo-hexanecarboxylic acid 1.0 g (4.15 mmol) and [3,5-bis-(4-cyano-phenoxy)-phenyl]-amine (1.34 g, 4.15 mmol) were used to afford 1.5 g of the required product. 1H NMR (DMSO-d6): δ 1.4 (9H, s), 2.3 (4H, m), 2.81 (1H, m), 3.15 (4H, m), 3.5 (1H, m), 6.71 (1H, s), 6.81 (1H, brs), 7.21 (6H, m), 7.92 (4H, d), 10.0 (1H, brs).

情報源と証拠